LC/MS/MS  workshop on environmental  applications  and food safety




ИмеLC/MS/MS  workshop on environmental  applications  and food safety
Дата на преобразуване09.11.2012
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източникhttp://www.idaea.csic.es/barcelona/final program-1.docx

8th  ANNUAL 

LC/MS/MS  WORKSHOP ON ENVIRONMENTAL  APPLICATIONS  AND FOOD SAFETY

2-4 July 2012, Barcelona, Spain


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MONDAY, 2nd July 2012


8.45 – 9.15 Registration


9.15 – 9.30 Welcome and Introduction

David Serrat, President of the Science and Technology Section, Institut d’Estudis Catalans, Barcelona, Spain

Damià Barceló, IDAEA-CSIC, Barcelona and ICRA, Girona, Spain


Session 1: Analytical challenges and new trend in LC-MS-MS


Chair: Damià Barceló


9.30 – 10.00 Novel micro and nano bioaffinity mass spectrometry tools for the detection of emerging contaminants in food and environment

Michel W.F. Nielen, RIKILT-Institute of Food Safety and Wageningen University, Wageningen, The Netherlands


10.00 – 10.30 Harnessing the potential of ion-mobility mass spectrometry for the development and characterization of a multi-residue method for the determination of veterinary antibiotics in crude extracts

Sandra Rontree, Waters Corporation, Manchester, UK


10.30 – 11.30 Poster session/Coffee break


Chair: Sandra Rontree


11.30 – 12.00 Reference Materials for Environmental and Food Analyses – LC/MS/MS in Their Development and Use

Stephen A. Wise, National Institute of Standards and Technology (NIST),

Gaithersburg, USA


12.00 – 12.30 Strategies for the Effective Integration of Reference Data and Reference Materials for MS Applications in Health and Environment

Carlos Gonzalez, National Institute of Standards and Technology (NIST),

Gaithersburg, USA


12.30 – 13.00 Doping for sensitivity: evaluation of atmospheric pressure photoionization (APPI) for the detection of wastewater related chemicals in aqueous samples

Piero R. Gardinali, Florida International University, Miami, Florida, USA.


13.00 – 13.30 Analytical challenges in high performance liquid chromatography tandem mass spectrometry for accurate determination of primary and secondary phthalate metabolites in real samples

Maria Jose Gonzalez, General Organic Chemistry Institute (CSIC), Madrid, Spain


13.30 – 15.30 Lunch


Session 2: Target analysis, non-target analysis, screening


Chair: Diana Aga


15.30 – 16.00 Enantiomeric profiling of chiral drugs in the environment with the usage of Chiral-LCMS/MS

Barbara Kasprzyk-Hordern, Department of Chemistry, University of Bath, UK


16.00 – 16.30 From target to non-target screening of micropollutants in the aquatic environment by HPLC combined with high resolution mass spectrometry

Juliane Hollender, EAWAG, Dübendorf , Switzerland


16.30 – 17.00 Significance of “known unknowns” analysis in water treatment

Jelena Radjenovic, The Advanced Water Management Centre (AWMC), Brisbane, Australia

.


17.00 – 17.40 Poster session/Coffee break


Chair: Frank L. Dorman


17.40 – 18.00 Liquid chromatography coupled to tandem mass spectrometry: triple quadrupole (QqQ) or quadrupole-time of flight (QTOF) detection for environmental applications?
Margoum Christelle,, Irstea, Lyon, France


18.00 – 18.20 Determination of endocrine disruptors and related compounds in river sediments by Turbulent-Flow Chromatography-LC-MS/MS

Marina Gorga, IDAEA-CSIC, Barcelona, Spain


18.20 – 18.40 Determination of pharmaceuticals in fish: method optimization and occurrence in different species from Mediterranean rivers

Belinda Huerta, ICRA, Girona, Spain


18.40 – 19.00 Development of analytical method based on ultra performance liquid chromatography (UPLC) tandem QTRAP mass spectrometry for determination of antihelmintic drugs in surface waters

Mirta Zrnčić, FKIT, University of Zagreb, Croatia


19.00 Asamblea del SEEM (Annual meeting of Spanish Society of Mass Spectrometry)




TUESDAY, 3rd July 2012


Session 3: Applications in environmental analysis


Chair: Amadeo Rodríguez Fernández-Alba




9.00 – 9.30 Occurrence and Fate of Pharmaceuticals and Personal Care Products in Municipal Wastewater Treatment Systems

Mehran Alaee, National Water Research Institute, Burlington, Canada


9.30 – 10.00 Solid-phase extraction - UHPLC-MS-MS for the analysis of polar organic persistent pollutants in coastal and marine waters for the implementation of the European Water Framework and Marine Strategy Framework Directives,

Robert Loos, European Commission - DG Joint Research Centre (JRC) Institute for Environment and Sustainability (IES), ISPRA, Italy


10.00 – 10.30 Investigation of pharmaceutical metabolites/transformation products in urban waste- water by LC-QTOF MS

Juan Vicente Sancho Llopis, University Jaume I, Castellón, Spain


10.30 – 11.30 Poster session/Coffee break


Chair: Mira Petrovic


11.30 – 12.00 Identification of Pharmaceutical By-products After Advanced Oxidation and Biofiltration of Wastewater

Diana S. Aga, Chemistry Department, University at Buffalo, Buffalo, NY, USA


12.00 – 12.30 Identifying the photoproducts of (demethyl)sildenafil: electrospray-high resolution MS/MS alone is not enough

Sandra Perez, IDAEA-CSIC, Barcelona, Spain


12.30 – 13.00 HILIC in service of low detection limits for X-ray contrast media

Bozo Zonja, IDAEA-CSIC, Barcelona, Spain


9.00 – 13.00 Parralel sesion: Rapid and efficient detection of contaminants in food using instrumental and bioanalytical methods

Highlights from research achievements within the FP7 EU project CONtaminants in Food and Feed: Inexpensive DEtectioN for Control of Exposure (CONffIDENCE),


13.00 – 15.00 Lunch


Chair: Marinella Farré


15.00 –15.30 Sources and analysis of polyfluorinated surfactants and related ´emerging´ fluorinated contaminants

Jana Hajslova, Institute of Chemical Technology, Prague, Czech Republic


15.30 – 16.00 Perfluorinated compounds determination by quadrupole time of flight mass time-of-spectrometry in environmental and food matrices

Yolanda Picó, Faculty of Pharmacy, University of Valencia, Spain


16.00 – 16.20 On-line SPE optimisation for the analysis of perfluorocarboxylic and perfluorosulfonic acids in surface and drinking waters by LC/MS/MS

Stefano Polesello, Water Research Institute CNR-IRSA, Brugherio (MB), Italy


16.20 – 16.40 Analysis of perfluoroalkyl substances in waters from Germany and Spain

Marta Llorca, IDAEA-CSIC, Barcelona and ICRA, Girona, Spain




16.40 – 17.00 Distribution of fluoroalquil substances on human body

Francisca Pérez, IDAEA-CSIC, Barcelona, Spain


17.00 – 17.40 Poster session/Coffee break


Chair: Mehran Alaee


17.40 – 18.00 Exact mass measurement at high resolution for identification, quantification and confirmation of poly(amidoamine) dendrimers (pamam) by LC-ESI-TRIPLE-TOF mass spectrometer

Maria Malgorzata Ulaszewska, IMDEA-Agua (Instituto Madrileño De Estudios Avanzados- Agua), Alcalá de Henares, Madrid, Spain


18.00 – 18.20 Analysis of volatile dimethylsiloxanes in wastewater, surface water, river sediment and biota samples

Josep Sanchís, IDAEA-CSIC, Barcelona, Catalonia, Spain


18.20 – 19.00 Simultaneous determination of HBCD isomers and TBBPA in biota

Guillaume ten Dam, RIKILT – Institute of Food Safety, Wageningen, The Netherlands




21.00 Joint dinner


WEDNESDAY, 3rd July 2012


Session 4: Applications in food analysis and forensics


Chair: Yolanda Picó




9.00 – 9.30 Benefits and pitfalls in the evaluation of pesticide residues in food by LC-QTOF-MS

Amadeo Rodríguez Fernández-Alba, University of Almeria, Almeria, Spain


9.30 – 10.00 Challenges in the Analysis of Residues from Packaging Materials in Food

Maria Teresa Galceran, University of Barcelona, Barcelona, Spain


10.00 – 10.30 New Ultra Performance Convergence Chromatography UPC2 combined with Analytical SFE for Food Safety

Helene Boiteux, Waters Corporation, St-Quentin, France


10.30 – 11.10 Poster session/Coffee break


Chair: Michel W.F. Nielen


11.10 – 11.40 Utilizing Serially-Coupled HPLC Columns and Elevated Temperature to Increase the Separation Efficiency of Cacao Metabolites

Frank L. Dorman, The Pennsylvania State University and Restek Corporation, USA


11.40 – 12.00 Comprehensive bioaffinity mass spectrometry approach for thyroid transporter agonists

Payam Aqai, RIKILT- Institute of Food Safety, Wageningen, The Netherlands


12.00 – 12.20 Chromatographic Analysis of Synthetic Amphetamine Street Samples

Amanda Leffler, The Pennsylvania State University, USA


12.20 – 12.40 Utilizing QTOF Screening for Pesticide Residue Analysis

Antonietta Gledhill, Waters Corporation, Manchester , UK


12.40 - 13.10 Micro pollutants as chemical markers for environmental forensics applications: Differentiating sewage and manure

Cecilia Fenech, School of Biotechnology, Dublin City University, Dublin, Ireland,


13.10 – 13.30 Discussion + student awards


13.30 End of workshop


Posters


Environmental



  1. Nanomaterials in the environment: Analysis of fullerenes in environmental matrixes and assessment of their acute toxicity effects in environmentally relevant conditions. Evidences of Trojan Horse Effect.

Josep Sanchís1, Naiara Berrojalbiz1, Gemma Caballero1, Jordi Dachs1,

Naif Abdullah Al-Harbi3, Marinella Farré1, Damià Barceló1,2,3

1 Department of Environmental Chemistry, IDAEA-CSIC, Barcelona, Catalonia, Spain

2 Catalan Institute for Water Research (ICRA), Girona, Catalonia, Spain

3 King Saud University, P.O. Box 2455, 11451, Riyadh, Saudi Arabia


  1. Multi-component quantitative analysis of pharmaceuticals and personal care products in the environment by LC-MS/MS with fast polarity switching

1Natsuyo Asano; 1Kiyomi Arakawa; 1Shinjiro Fujita; 1Kazuo Mukaibatake; 1Ichiro Hirano; 2Yuka Fujito

1Shimadzu Corporation: 1, Nishinokyo-Kuwabaracho Nakagyo-ku, Kyoto 604–8511, Japan

2Shimadzu Analytical and Measuring Center Inc.: 1, Shimoaicho Nishinokyo Nakagyo-ku, Kyoto 604-8436, Japan


  1. Application of mass spectrometry techniques for the determination of organic contaminants on food-processing industry effluents

M.M Gómez-Ramos, M. Mezcua, C. Ferrer, S. Uclés, A.R. Fernandez-Alba, A. Agüera

Pesticide Residue Research Group, University of Almería, Spain



  1. Simultaneous quantitative/qualitative screening of PPCPs in river water by LC-QTOF-MS and direct sample injection

Sonia Herrera1, Maria M. Ulaszewska1, MªJesús Martínez Bueno1,2, Amadeo R. Férnandez-Alba1,2

1 Fundación IMDEA-Agua, C/ Punto Net 4, 2ª planta, Edificio ZYE, Parque Científico Tecnológico de la Universidad de Alcalá. 28805, Alcalá de Henares. Madrid (Spain)

2 Pesticide Residues Research Group, Department of Hydrogeology and Analytical Chemistry, University of Almería, 04120 La Cañada de San Urbano, Almería (Spain)


  1. Towards more accurate environmental measurements. A case study on LC-MS2 pesticides quantification in water

Lardy-Fontan S., Le Diouron V., Lalere B., Vaslin-Reimann S.

Laboratoire National De Metrologie D’essais Lne, 1 Rue Gaston Boissier, 75724 Paris Cedex 15, France


  1. Analysis of trace level phthalate esters in environmental water samples by using online-SPE-LC coupled to a high speed triple quadrupole mass spectrometer

1Ichiro Hirano, 1 Tairo Ogura, 2Yuka Fujito

1Shimadzu Corporation: 1, Nishinokyo-Kuwabaracho Nakagyo-ku, Kyoto 604–8511, Japan

2Shimadzu Analytical and Measuring Center Inc.: 1, Shimoaicho Nishinokyo Nakagyo-ku, Kyoto 604-8436, Japan



  1. Characterization and estimation of sulfaquinoxaline metabolites in residue analysis using liquid chromatography coupled to tandem mass spectrometry

Rodrigo Barcellos Hoff*1,2, Fabiano Barreto1, Jéssica Melo1, Louise Jank1 , Maria do Carmo Ruaro Peralba2, Tânia Mara Pizzolato2

1 - Laboratório Nacional Agropecuário do Rio Grande do Sul (LANAGRO/RS), Porto Alegre, RS, Brazil.

2 Instituto de Química - Universidade Federal do Rio Grande do Sul, Porto Alegre, RS, Brazil.


  1. Antibiotics degradation by photolytic process in different water matrices

Carla Sirtoria,b, Louíse Janka, Flávia Justina Costaa, Tânia Mara Pizzolatoa

a Instituto de Química, Universidade Federal do Rio Grande do Sul (UFRGS), Av. Bento Gonçalves, 9500, Porto Alegre - RS, Brasil;

b Universidade Federal da Integração Latino-Americana (UNILA), Av. Tancredo Neves, 6731 - Bloco 4, Caixa Postal 2044 - CEP 85867-970, Foz do Iguaçu - PR, Brasil.


  1. Multiresidue trace determination of UV-absorbing compounds in fish using HPLC-(ESI)-QqLIT-MS2

Pablo Gago-Ferrero1*, M.Silvia Díaz-Cruz1, Damià Barceló1,2.

1Dept. Environmental Chemistry, IDAEA-CSIC, Jordi Girona 18-26, E-08034 Barcelona, Spain.

2Catalan Institute for Water Research (ICRA), Emili Grahit 101, Edifici H2O, Parc Científic i Tecnològic de la Universitat de Girona, 17003 Girona, Spain


  1. Hospital effluents as source of pharmaceuticals: characterization and contribution of four different hospitals

L.H.M.L.M. Santos1*, M. Gros2, S. Rodriguez-Mozaz2, D. Barceló2,3, C. Delerue-Matos4, A. Pena5, M.C.S.M.B. Montenegro1

1REQUIMTE, Departamento de Ciências Químicas, Faculdade de Farmácia da Universidade do Porto, Rua de Jorge de Viterbo, n.º 228, 4050-313 Porto, Portugal

2Catalan Institute for Water Research (ICRA), C/Emili Grahit 101, 17003 Girona, Spain

3IDAEA-CSIC: Department of Environmental Chemistry, IDAEA-CSIC, C/ Jordi Girona 18-26, 08034 Barcelona, Spain

4REQUIMTE, Instituto Superior de Engenharia do Porto, Rua Dr. António Bernardino de Almeida 431, 4200-072 Porto, Portugal

5 Group of Health Surveillance, Center of Pharmaceutical Studies, University of Coimbra, Health Sciences Campus, Azinhaga de Santa Comba, 3000-548 Coimbra, Portugal


  1. Selective pressurized liquid extraction and liquid chromatography tandem mass spectrometry for the analysis of alkylphenols and bisphenol a in mussels

N. Salgueiro-González, M. I. Turnes-Carou, S. Muniategui-Lorenzo, P. López-Mahía, D. Prada-Rodríguez. Department of Analytical Chemistry. University of A Coruña. Campus da Zapateira. E-15071 A Coruña, Spain





  1. Direct injection with triple quadrupole LC/MS system: rapid method for the analysis of PFOS and PFOA in water

Laura Díaz Esplá, , Lorena Sanjuan Tortosa, Julio Llorca Pórcel

LABAQUA S.A. c/ del Dracma, Parcelas 16-18 03114-Alicante, Spain


  1. Study of Diclofenac metabolic biotransformation pathways to its nitrified microbial metabolites and development of an LC-MS/MS method for their determination in wastewater.

Victoria Osorio1, Marta Imbert-Bouchard1, Asunción Navarro1, Jose Luis Abad2, Antoni Ginebreda2, Sandra Pérez1, Damià Barceló1,3

1 IDAEA-CSIC, Department of Environmental Chemistry, Jordi Girona 18-26, Barcelona (Spain),

2 RUBAM-IIQAC-CSIC Department of Biomedical Chemistry, Jordi Girona 18-26, Barcelona (Spain),

3 Catalan Institute for Water Research (ICRA), Parc Cientıfic i Tecnologic de la Universitat de Girona, Edifici Jaume Casademont, Porta A, Planta 1, Despatx 13C/ Pic de Peguera, 15E-17003 Girona, Spain


  1. Novel amide polar-embeded revesed-phase column for the fast liquid chromatography-tandem mass spectrometry determination of polyether ionophores in sewage and river waters

Pol Herrero, Francesc Borrull, Rosa Mª Marcé and Eva Pocurull

Department of Analytical Chemistry and Organic Chemistry, Faculty of Chemistry, Universitat Rovira I Virgili, C/ Marcel·lí Domingo s/n, 43007, Tarragona, Catalonia, Spain


  1. Residues and organic contaminants in agricultural soils in intensive agricultural areas from Spain: a three years survey

Lucía Alcarraz Farall1,2, Juan Antonio Padilla-Sánchez2, Roberto Romero-González2, Patricia Plaza-Bolaños2,3, José Luis Martínez Vidal2, Antonia Garrido Frenich2

1Tecnological Laboratory of Uruguay (LATU), Avenida Italia 6201, 11500. Montevideo (Uruguay)

2Research Group “Analytical Chemistry of Contaminants”, Department of Hydrogeology and Analytical Chemistry, Research Centre for Agricultural and Food Biotechnology (BITAL), University of Almeria, Agrifood Campus of International Excellence, ceiA3, Carretera de Sacramento s/n, E-04120, Almeria (Spain)

3Department of Analytical Chemistry, University of Granada, E-18071, Granada (Spain)


  1. Screening and quantifying anti-cancer drugs and metabolites in hospital’s wastewaters and rivers by online SPE – LC-MS/MS.

Mikaël Levi2, Claude Villard1, Thérèse Schembri1, Marcus Mreyen4, Anja Grüning4, Stéphane Moreau2, Pierre Boissery3, Daniel Lafitte2

1Aix Marseille Université, Inserm UMR 911 CRO2 faculté de pharmacie 27 bd jean moulin 13385 Marseille , France.

2 SHIMADZU France SAS, Le Luzard 2, Boulevard Salvador Allende, 77448 Marne la Vallée Cedex 2, France.

3 Agence de l'Eau Rhône Méditerranée & Corse, délégation de Marseille, 62 immeuble Le Noaille, 13001 Marseille, France.

4 SHIMADZU Europa GmbH, Albert-Hahn-Str. 6-10, D-47269 Duisburg, Germany.


  1. Simultaneous determination of ten different pharmaceuticals and three sulfonamide metabolites by high performance liquid chromatography -tandem mass spectrometry

Martina Periša, Sandra Babić

Department of Analytical Chemistry , Faculty of Chemical Engineering and Technology, Marulićev trg 19, 10000 Zagreb, Croatia


  1. Enantiomeric profiling of chiral drugs from environmental solid matrices with the use of microwave assisted extraction and chiral LC-MSMS


Sian Evans, Paul Davies, Anneke T. Lubben and Barbara Kasprzyk-Hordern

University of Bath, Department of Chemistry, Faculty of Science, Bath, BA2 7AY, UK

  1. Trametes versicolor degrades the antiepileptic carbamazepine: Identification of intermediates formed in an air pulsed fluidized bed bioreactor


Aleksandra Jelica, Carles Cruz-Moratób, Ernest Marco-Urreab, Monserrat Sarràb, Sandra Pereza ,Teresa Vicentb ,Mira Petrovic c, d ,Damia Barcelo a, d

a Department of Environmental Chemistry, Institute of Environmental Assessment and Water Research (IDAEA), Spanish Council for Scientific Research (CSIC), 08034 Barcelona, Spain

b Departament d’Enginyeria Química, Universitat Autònoma de Barcelona (UAB), Bellaterra, Spain

c Institució Catalana de Recerca i Estudis Avançats (ICREA), Barcelona, Spain

d Catalan Institute for Water Research (ICRA), H2O Building, Scientific and Technological Park of the University of Girona, Girona, Spain



  1. Rapid screening and confirmation of emerging contaminants in UK river waters by UHPLC-IT-TOF

David R. Baker1, John Bagnall2, Alan J. Barnes1, Barbara Kasprzyk-Hordern2, Neil J. Loftus1

1Shimadzu, Manchester, UK; 2University of Bath, Bath, UK


  1. Liquid chromatography-tandem mass spectrometry to determine sweeteners in wastewater and surface water

P. Arbeláez, F. Borrull, E. Pocurull, R. M. Marcé

Department of Analytical Chemistry and Organic Chemistry, Universitat Rovira i Virgili, Marcel.lí Domingo s/n 43007 Tarragona, Spain


  1. LC-MS-MS to determine phosphodiesterase type V inhibitors, analogues and their metabolites in different water matrices

Jaume Aceña1, Bianca Ferreira da Silva2, J.L Abad3, Sandra Pérez1, Damià Barceló1,4

1 IDAEA-CSIC, Department of Environmental Chemistry, Jordi Girona 18-26, Barcelona (Spain),

2 Laboratório de Biogeoquímica Ambiental, Department of Chemistry, UFSCar, Rod. Wash. Luís km235, São Carlos, SP, Brazil

3 IQAC-CSIC, Jordi Girona 18-26, Barcelona (Spain),

4 Catalan Institute for Water Research- ICRA, C/Emili Grahit, 101, Edifici H2O, Parc Científic i Tecnològic de la Universitat de Girona, E-17003 Girona, Spain


  1. Simultaneous Quantitative Analysis of Pesticides Including Phenoxy-Acids in Surface Water using UPLC-MS/MS with direct injection
    Gerard Bondoux, Waters Corporation,




  1. Determination of wetland pollutants by liquid chromatography-tandem mass spectrometry
    Pablo Vazquez-Roig1, Cristina Blasco1, Vicente Andreu2, Yolanda Picó1
    1 Grupo de Investigación en Seguridad Alimentaria y Medioambiental (SAMA-UV), Facultat de Farmàcia, Universitat de València, Av, Vicent Andrés s/n, 46100 Burjassot, València, España.
    2




  1. Levels of perfluorinated contaminants in breast milk of the Valencian community by liquid chromatography-tandem mass spectrometry

C. Blasco1*, Y. Picó1, A. Masiá1, M. Farré2, D. Barceló2

1 Grupo de Investigación en Seguridad Alimentaria y Medioambiental (SAMA-UV), Facultat de Farmàcia, Universitat de València, Av, Vicent Andrés s/n, 46100 Burjassot, València, España.

2 Department of Environmental Chemistry, IDAEA-CSIC,C/Jordi Girona 18-26, Barcelona, España


26. Outcompeting GC for the detection of legacy chlorinated pesticides: online-SPE UPLC APCI/MSMS detection of endosulfans at part per tillion levels.

Natalia Quinete1 and Piero Gardinali1,2

1Southeast Environmental Research Center (SERC) and 2Department of Chemistry and Biochemistry, Florida International University, 3000 NE 151 Street, Biscayne Bay Campus, North Miami, Florida,33181 USA.


  1. Development of a liquid/electrospray chemical ionization tandem mass spectrometry analytical method for analysis of eleven hydroxylated polybrominated diphenyl ethers.

Maria Luisa Feo1, Enrique Baron1, Diana S. Aga2, Ethel Eljarrat1, Damiá Barcelò1,3.

1 IDEA CSIC, Analytical Chemistry Department, Jordi Girona 18-26, 08034 Barcelona, Spain.

2Department of Chemistry, University at Buffalo, State University of New York, Buffalo, New York 14260.

3 Catalan Institute for Water Research (ICRA), Parc Científic i Tecnològic de la Universitat de Girona, Pic de Peguera 15, 17003 Girona, Spain


  1. The stereo-selective biodegradation of amphetamine and methamphetamine in river water using chiral-LC-(QTOF)MS

John Bagnall, Louis Malia, Anneke Lubben and Barbara Kasprzyk-Hordern

University of Bath, Department of Chemistry, Faculty of Science, Bath, BA2 7AY, UK


  1. Analysis of Synthetic Cannabinoids using GC-MS and LC-MS/MS

Sharyn E. Miller, The Pennsylvania State University


  1. Selection of a Column and Optimization of a method for the Analysis of Antidepressants in Aqueous Samples using Liquid Chromatography-Tandem Mass Spectrometry

Kenton Chodara, The Pennsylvania State University

31. LC-MS/MS and Accelerated Solvent Extraction (ASE) Pesticide Residues Analysis in Sediments from Botafogo River, PE-Brazil

Rodrigues, H.O.S.; Silva, H.C.M.P.; Cunha, A.N; Albuquerque Junior, E.C*.; Telles, D.L.; Araujo, A.C.P.

Institute of Technology of Pernambuco – ITEP. Laboratory of Pesticide Residue Analysis – LabTox. Pernambuco-Brazil. 50740-540


Food and forensics



  1. Rapid method for the detection of metabolite of nerve agents in urine by liquid chromatography–negative electrospray-tandem mass spectrometry

Arkady Braun1, Igor Rodin1, Oleg Shpigun1, Andrey Stavrianidi1, Igor Rybalchenko2

1. Department of Chemistry, Lomonosov Moscow State University, Moscow, Russia.

2. Lumex ltd, Moscow, Russia


  1. Quick target scan of LC screening method for pesticides analysis in fruits and vegetables

Samanta Uclés, Ana Uclés, Carmen Ferrer, Ana Agüera, Amadeo R. Fernández-Alba

Pesticide Residue Research Group, Dpt. of Hydrogeology and Analytical Chemistry

University of Almería, Ctra. Sacramento s/n, 04120 Almería, Spain


  1. Analysis of poly(amidoamine) dendrimers (PAMAM) in biological samples by LC-QLIT-MS/MS

Ana Uclés 1,2, MªJesús Martínez Bueno1,2, María Dolores Hernando3, Amadeo R. Férnandez-Alba1,2

1Fundación IMDEA-Agua, C/ Punto Net 4, 2ª planta, Edificio ZYE, Parque Científico Tecnológico de la Universidad de Alcalá. 28805, Alcalá de Henares. Madrid (Spain)

2 Pesticide Residues Research Group, Department of Hydrogeology and Analytical Chemistry, University of Almería, 04120 La Cañada de San Urbano, Almería (Spain)

3 Spanish National Institute for Agriculture and Food Research and Technology, INIA, Crta. de la Coruña, km. 7,5 28040 Madrid (Spain)


  1. Rapid and Highly Sensitive Quantitative Analysis and Screening of Aflatoxins in Foods Using Liquid Chromatography Triple Quadrupole Mass Spectrometry

1Manami Kobayashi; 1Satoshi Yamaki; 1Ayako Nomura; 1Kyoko Watanabe; 1YoshihiroHayakawa; 1Tsutomu Nishine; 2Yuka Fujito

1Shimadzu Corporation: 1, Nishinokyo-Kuwabaracho Nakagyo-ku, Kyoto 604–8511, Japan

2Shimadzu Analytical and Measuring Center Inc.: 1, Shimoaicho Nishinokyo Nakagyo-ku, Kyoto 604-8436, Japan


  1. Identification of amoxicillin, ceftiofur and cephapirin metabolites and transformation products in chicken muscle by LC-ESI-QTOF-MS/MS

P. Gómez-Rodríguez, M.P. Hermo, J.Barbosa, D. Barrón

University of Barcelona, Faculty of Chemistry, Department of Analytical Chemistry, Diagonal 645, E- 08028 Barcelona (Spain)


  1. Standard-free qualitative analysis of ginsenosides in plants by HPLC-MS/MS

Stavrianidi Andrey, Rodin Igor, Braun Arkady, Shpigun Oleg.

Chemistry Department, Lomonosov Moscow State University, Moscow, Russia


  1. Simultaneous HPLC-MS/MS determination of salidroside, rosarin and rosavin in the extracts from Rhodiola rosea

Rodin Igor, Stavrianidi Andrey, Braun Arkady, Shpigun Oleg

Chemistry Department, Lomonosov Moscow State University, Moscow, Russia


  1. LC-MS/MS method for simultaneous determination of anaplerotic dysfunction, methylmalonic acidemia and endothelial dysfunction metabolic markers in human plasma

A. Stavrianidi1, A. Braun1, I. Ananieva1, I. Rodin1, O. Shpigun1, A. Zhloba2

1. Chemistry Department, Lomonosov Moscow State University, Moscow, Russia

2. St.-Petersburg State I.P. Pavlov Medical University, Petersburg, Russia


  1. Exploring the application of a universal method for pesticide screening in foods using a high data acquisition speed MS/MS

1Ichiro Hirano, 1Yusuke Inohana, 1Kiyomi Arakawa, 2Yuka Fujito

1Shimadzu Corporation: 1, Nishinokyo-Kuwabaracho Nakagyo-ku, Kyoto 604–8511, Japan

2Shimadzu Analytical and Measuring Center Inc.: 1, Shimoaicho Nishinokyo Nakagyo-ku, Kyoto 604-8436, Japan


  1. Multi-class pesticides residues analysis in challenging vegetable matrices by using fast MRM with 15 msec polarity switching

1Ichiro Hirano, 1Kiyomi Arakawa, 1Yusuke Inohana, 2Yuka Fujito

1Shimadzu Corporation: 1, Nishinokyo-Kuwabaracho Nakagyo-ku, Kyoto 604–8511, Japan

2Shimadzu Analytical and Measuring Center Inc.: 1, Shimoaicho Nishinokyo Nakagyo-ku, Kyoto 604-8436, Japan


  1. High Throughput Quantitative Analysis of Multi-mycotoxin in Beers using UHPLC-MS/MS

Masayoshi Tamura 1; Keiko Matsumoto 2; Jun Watanabe 2; Junko Iida 2; Yuka Fujito3;

Yasushi Nagatomi 1; Naoki Mochizuki 1;

  1. Asahi Group Holdings, Limited, 1-1-21 Midori, Moriya, Ibaraki 302–0106, Japan

  2. Shimadzu Corporation. 1, Nishinokyo-Kuwabaracho Nakagyo-ku, Kyoto 604–8511, Japan

  3. Shimadzu Analytical & Measuring Center Inc. , 1, Shimoaicho Nishinokyo Nakagyo-ku, Kyoto 604-8436, Japan




  1. Simultaneous identification, confirmation and quantification of pesticides and veterinary drug residues in meat matrices applying a high resolution mass database

María Luz Gómez-Pérez1, Patricia Plaza-Bolaños1,2, Roberto Romero-González1, José Luis Martínez Vidal1, Antonia Garrido Frenich1

1Research Group “Analytical Chemistry of Contaminants”, Department of Hydrogeology and Analytical Chemistry, Research Centre for Agricultural and Food Biotechnology (BITAL), University of Almeria, Agrifood Campus of International Excellence, ceiA3, Carretera de Sacramento s/n, E-04120, Almeria (Spain)

2Department of Analytical Chemistry, University of Granada, E-18071, Granada (Spain)


  1. Occurrence of cloxacillin and ampicillin in cow milk after the end of the withdrawal period of dry cow intramammary antibiotics

Erja Lindfors1, Katariina Pekkanen2, Kaija-Leena Saraste3

Finnish Food Safety Authority Evira, 1Chemistry and Toxicology Research Unit, 2Food and Feed Microbiology Research Unit. 3Food Hygiene Unit. Mustialankatu 3, FI-00790, Helsinki, Finland


  1. Multi-residue quantitation of veterinary drugs in animal tissue using an optimised solid phase extraction protocol.

1Alan J. Barnes, 3Yuka Fujito, 2Ichiro Hirano, 1Neil J. Loftus

1Shimadzu Corporation, MS-BU Overseas, Manchester, United Kingdom; 2Shimadzu Corporation: 1, Nishinokyo-Kuwabaracho Nakagyo-ku, Kyoto 604–8511, Japan; 3Shimadzu Analytical and Measuring Center Inc.: 1, Shimoaicho Nishinokyo Nakagyo-ku, Kyoto 604-8436, Japan


  1. Multiclass method for determination of 27 pesticides in food and soil samples by LC-MS/MS

Virgínia C. Fernandes (1,2)*, Steven Lehotay (3), L. Geis-Asteggiante (3) , V.F. Domingues (1), N. Mateus (2) and C. Delerue-Matos (1)

(1) REQUIMTE – Instituto Superior de Engenharia, Instituto Politécnico do Porto, Portugal

(2) CIQ – Centro de Investigação em Química, Universidade do Porto, Portugal

(3) Eastern Regional Research Center, Agricultural Research Service, U.S. Department of Agriculture, Wyndmoor, PA. USA


  1. The use of Microflow UHPLC as a way to solvent usage in pesticide screening of food samples by LC-MS/MS

Stephen Lock and Pam Stoddart

AB SCIEX, Warrington, Cheshire, UK


  1. The use of large volume injection as a way to reduce sample preparation in pesticide screening of drinking water and other beverages by LC-MS/MS

Stephen Lock and Pam Stoddart

AB SCIEX, Warrington, Cheshire, UK


  1. New approaches for Screening and Quantitation of Mycotoxins in different baby food Matrices

Stephen Lock, Jianru Stahl-Zeng and Kristin von Czapiewski,

AB SCIEX, Pheonix House, Centre Park, Warrington, UK


  1. Can LC/MS/MS be used as a routine tool for Allergens analysis including the detection of Mustard?  

Stephen Lock

AB SCIEX, Warrington, Cheshire, UK


  1. Comprehensive Analysis of the B-Vitamin Complex in Food and Beverages by LC-MS/MS

Stephen Lock

AB SCIEX, Pheonix House, Centre Park, Warrington, UK


  1. Extraction of fluoroquinolones fom eggs using molecularly imprinted polymers

Cristina Blasco and Yolanda Picó,
University of Valencia, Spain


  1. Determination of plasma metabolites of thyme bioactive compounds by improved liquid chromatography coupled to tandem mass spectrometry

Alba Macià, Laura Rubió, Aida Serra, Maria-Paz Romero, Maria-José Motilva

Food Technology Department, Escola Tècnica d’Enginyeria Superior Agrària, Universitat de Lleida. Av. Alcalde Rovira Roure, 191. 25198 Lleida. Spain.


  1. Pesticide and veterinary drugs residue analysis in goat milk

Porto Filho JM1; Costa RG1; Cunha NA2; Silva MCC2; Silva HCM2; Albuquerque Junior EC2, Silva M2;Telles DL2, Araújo ACP2

1Federal University of Paraiba - UFPB, Areia CCA Zootecnic Doctorate Program. Areia-PB-BRAZIL.

2Pesticide Residue Laboratory - LabTox/ITEP, Av. Prof. Luis Freire 700. 50740-540. Recife-PE-BRAZIL


54. Analysis of fluorotelomer alcohols (FTOHs) in food contact materials

Darina Lanková, Jana Pulkrabová, Ondřej Lacina, Michala Kočkovská, Jana Hajšlová

Institute of Chemical Technology Prague, Department of Food Analysis and Nutrition, Technická 3, Prague 6, 166 28, Czech Republic

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